产品详情
- Molecular Formula:C13H15FN2O2
- Molecular Weight:250.273
182182-31-6 Relevant articles
Intermediate for synthesizing camptothecin derivative as well as preparation method and application thereof
-
, (2020/08/09)
The invention relates to the technical f...
Aminotetralone derivatives and preparation process thereof
-
, (2008/06/13)
The present invention pertains to a proc...
182182-31-6 Process route
-
- 143655-70-3
C15H17FN2O3
-
- 182182-31-6
2-Acetylamino-8-amino-6-fluoro-5-methyl-1-tetralone
Conditions
| Conditions | Yield |
|---|---|
|
With hydrogenchloride; In methanol; at 60 ℃; for 0.5h; Inert atmosphere;
|
93% |
-
-
C13H16FNO2
-
- 182182-31-6
2-Acetylamino-8-amino-6-fluoro-5-methyl-1-tetralone
Conditions
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 3 steps
1.1: dipotassium peroxodisulfate / acetonitrile; water / 8 h / 30 °C
2.1: potassium tert-butylate / tetrahydrofuran; tert-butyl alcohol / 0.17 h / 5 °C
2.2: 1 h
3.1: hydrogenchloride / methanol / 0.5 h / 60 °C / Inert atmosphere
With hydrogenchloride; dipotassium peroxodisulfate; potassium tert-butylate; In tetrahydrofuran; methanol; water; acetonitrile; tert-butyl alcohol;
|
182182-31-6 Upstream products
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143655-70-3
C15H17FN2O3
-
452-77-7
3-fluoro-4-methyl-phenylamine
-
458-10-6
N-(3-fluoro-4-methylphenyl)acetamide
-
202865-76-7
C9H9BrFNO
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