产品详情
- Molecular Formula:C22H25N3O6
- Molecular Weight:427.457
157896-03-2 Relevant articles
AN EFFICIENT AND SCALABLE PROCESS FOR THE MANUFACTURE OF FONDAPARINUX SODIUM
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Page/Page column 39; 61, (2013/08/15)
The present invention relates to a proce...
EFFICIENT AND SCALABLE PROCESS FOR THE MANUFACTURE OF FONDAPARINUX SODIUM
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Page/Page column 33, (2012/05/20)
The present invention relates to a proce...
A synthetic approach to aromatic aminoglycoside as a neamine mimic
Inoue, Ryo,Matsuda, Sho,Oda, Yoshiki,Ooyama, Hirofumi,Yoshida, Akihiro,Hamasaki, Keita,Yamanoi, Takashi
experimental part, p. 1335 - 1343 (2012/03/27)
This paper describes the synthetic appro...
PROCESS FOR PREPARING FONDAPARINUX SODIUM AND INTERMEDIATES USEFUL IN THE SYNTHESIS THEREOF
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Page/Page column 35, (2011/05/08)
Processes for the synthesis of the Facto...
157896-03-2 Process route
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- 55682-48-9
1,6-anhydro-2-azido-3,4-di-O-benzyl-2-deoxy-D-glucopyranose
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- 157896-03-2
6-O-Acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranose
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 2 steps
1: boron trifluoride diethyl etherate / dichloromethane / 3 h / -10 - 20 °C / Industry scale; Inert atmosphere
2: hydrazinium monoacetate / N,N-dimethyl-formamide / 3 h / 20 °C / Industry scale
With boron trifluoride diethyl etherate; hydrazinium monoacetate; In dichloromethane; N,N-dimethyl-formamide;
|
|
|
Multi-step reaction with 2 steps
1: boron trifluoride diethyl etherate / dichloromethane / -10 - 20 °C / Inert atmosphere
2: hydrazinium monoacetate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
With boron trifluoride diethyl etherate; hydrazinium monoacetate; In dichloromethane; N,N-dimethyl-formamide;
|
|
|
Multi-step reaction with 2 steps
1: boron trifluoride diethyl etherate / dichloromethane / -10 - 20 °C / Inert atmosphere; Large scale
2: hydrazinium monoacetate / N,N-dimethyl-formamide / -10 - 20 °C / Large scale
With boron trifluoride diethyl etherate; hydrazinium monoacetate; In dichloromethane; N,N-dimethyl-formamide;
|
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- 133076-39-8
1,6-di-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranose
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- 157896-03-2
6-O-Acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranose
| Conditions | Yield |
|---|---|
|
With hydrazinium monoacetate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
|
100% |
|
With hydrazinium monoacetate; In N,N-dimethyl-formamide; at -10 - 20 ℃; Large scale;
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100% |
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With hydrazinium monoacetate; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Industry scale;
|
98% |
157896-03-2 Upstream products
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136172-58-2
1,6-di-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α,β-D-glucopyranose
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245109-97-1
thexyldimethylsilyl 6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranoside
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171032-74-9
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-D-glucopyranose
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157488-88-5
thexyldimethylsilyl 2-azido-2-deoxy-β-D-glucopyranoside
157896-03-2 Downstream products
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133076-40-1
6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranosyl trichloroacetimidate
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154970-28-2
6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl trichloroacetimidate
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245110-04-7
allyl O-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-methyl-3-O-benzyl-α-L-idopyranosiduronate
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245110-06-9
allyl (6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-methyl-3-O-benzyl-α-L-idopyranosiduronate
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