产品详情
- Molecular Formula:C28H30O6S
- Molecular Weight:494.609
1352561-81-9 Relevant articles
PREPARATION OF MONOSACCHARIDES, DISACCHARIDES, TRISACCHARIDES, AND PENTASACCHARIDES OF HEPARINOIDS
-
, (2017/02/02)
The present invention provides preparati...
Total synthesis of anticoagulant pentasaccharide fondaparinux
Li, Tiehai,Ye, Hui,Cao, Xuefeng,Wang, Jiajia,Liu, Yonghui,Zhou, Lifei,Liu, Qiang,Wang, Wenjun,Shen, Jie,Zhao, Wei,Wang, Peng
, p. 1071 - 1080 (2014/05/20)
The anticoagulant pentasaccharide fondap...
Exploring and exploiting the reactivity of glucuronic acid donors
De Jong, Ana-Rae,Hagen, Bas,Van Der Ark, Vincent,Overkleeft, Herman S.,Codee, Jeroen D. C.,Van Der Marel, Gijsbert A.
, p. 108 - 125 (2012/03/07)
The relative reactivity of glucuronic ac...
1352561-81-9 Process route
-
- 850416-39-6
p-methylphenyl 2,3-di-O-benzyl-4,6-O-(R)-benzylidene-1-thio-β-D-glucopyranoside
-
- 1352561-81-9
C28H30O6S
Conditions
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 3 steps
1: trifluoroacetic acid / dichloromethane; water / 0.33 h / 20 °C
2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 5 h / 20 °C
3: potassium hydrogencarbonate / N,N-dimethyl-formamide / 4 h / 0 - 20 °C
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; potassium hydrogencarbonate; trifluoroacetic acid; In dichloromethane; water; N,N-dimethyl-formamide;
|
-
- 67-56-1
methanol
-
-
C27H28O6S
-
- 1352561-81-9
C28H30O6S
Conditions
| Conditions | Yield |
|---|---|
|
With sulfuric acid; at 55 ℃;
|
4.51 g |
1352561-81-9 Upstream products
-
74-88-4
methyl iodide
-
596087-18-2
4-methylphenyl 2,3-di-O-benzyl-1-thio-β-D-glucopyranoside
-
219518-19-1
4-methylphenyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside
-
850416-39-6
p-methylphenyl 2,3-di-O-benzyl-4,6-O-(R)-benzylidene-1-thio-β-D-glucopyranoside
1352561-81-9 Downstream products
-
1352561-84-2
C51H56O13
-
1352561-50-2
C30H32O7S
-
87907-01-5
methyl (2,3-di-O-benzyl-4-O-chloroacetyl-α-D-glucopyranosyl bromide)uronate
-
87907-02-6
O-(methyl 2,3-di-O-benzyl-4-O-(chloroacetyl)-β-D-glucopyranosyluronate)-(1->4)-3-O-acetyl-1,6-anhydro-2-azido-2-deoxy-β-D-glucopyranose
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