1286730-01-5
- Product Name：Pharmaceutical Intermediates intermediate
- Structural Formula：
- Purity：99%
- Molecular Weight：410.41
Product Details
Factory Supply Pharmaceutical Intermediates Pharmaceutical Intermediates intermediate 1286730-01-5 Manufacturer
- Molecular Formula:C13H14F2N4OS*(x)H2O4S
- Molecular Weight:410.41
1286730-01-5 Relevant articles
Process for the manufacture of enantiomerically pure antifungal azoles as ravuconazole and isavuconazole
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Page/Page column 9, (2011/04/25)
A new technical process for preparation ...
1286730-01-5 Process route
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241479-74-3
(2S,3R)-3-(2,5-difluorophenyl)-3-hydroxy-2-methyl-4-(1H-1,2,4-triazol-1-yl)butyronitrile
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1286730-01-5
(2R,3R)-3-(2,5-difluorophenyl)-3-hydroxy-2-methyl-4-(1H-1,2,4-triazol-1-yl)thiobutyramide hydrogensulphate
Conditions
| Conditions | Yield |
|---|---|
|
With
sulfuric acid; hydrogen sulfide;
In
ethanol;
for 5h;
Autoclave;
Heating;
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3-(2,5-difluorophenyl)-3-hydroxy-2-methyl-4-(1H-1,2,4-triazol-1-yl)butanenitrile
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1286730-01-5
(2R,3R)-3-(2,5-difluorophenyl)-3-hydroxy-2-methyl-4-(1H-1,2,4-triazol-1-yl)thiobutyramide hydrogensulphate
Conditions
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 3 steps
1: acetone; methanol / 20 °C / Reflux
2: sodium hydroxide / dichloromethane; water
3: hydrogen sulfide; sulfuric acid / ethanol / 5 h / Autoclave; Heating
With
sulfuric acid; hydrogen sulfide; sodium hydroxide;
In
methanol; ethanol; dichloromethane; water; acetone;
|
1286730-01-5 Upstream products
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241479-74-3
(2S,3R)-3-(2,5-difluorophenyl)-3-hydroxy-2-methyl-4-(1H-1,2,4-triazol-1-yl)butyronitrile
Relevant Products
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3,3A,6,6A-TETRAHYDROCYCLOPENTA[B]FURAN-2-ONECAS：34638-25-0
